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<front>
<journal-meta>
<journal-id journal-id-type="pmc">FDMP</journal-id>
<journal-id journal-id-type="nlm-ta">FDMP</journal-id>
<journal-id journal-id-type="publisher-id">FDMP</journal-id>
<journal-title-group>
<journal-title>Fluid Dynamics &#x0026; Materials Processing</journal-title>
</journal-title-group>
<issn pub-type="epub">1555-2578</issn>
<issn pub-type="ppub">1555-256X</issn>
<publisher>
<publisher-name>Tech Science Press</publisher-name>
<publisher-loc>USA</publisher-loc>
</publisher>
</journal-meta>
<article-meta>
<article-id pub-id-type="publisher-id">52398</article-id>
<article-id pub-id-type="doi">10.32604/fdmp.2024.052398</article-id>
<article-categories>
<subj-group subj-group-type="heading">
<subject>Article</subject>
</subj-group>
</article-categories>
<title-group>
<article-title>Stability of a Viscous Liquid Film in a Rotating Cylindrical Cavity under Angular Vibrations</article-title><alt-title alt-title-type="left-running-head">Stability of a Viscous Liquid Film in a Rotating Cylindrical Cavity under Angular Vibrations</alt-title><alt-title alt-title-type="right-running-head">Stability of a Viscous Liquid Film in a Rotating Cylindrical Cavity under Angular Vibrations</alt-title>
</title-group>
<contrib-group>
<contrib id="author-1" contrib-type="author" corresp="yes">
<name name-style="western"><surname>Kozlov</surname><given-names>Victor</given-names></name>
<xref ref-type="aff" rid="aff-1">1</xref><email>kozlov@pspu.ru</email>
</contrib>
<contrib id="author-2" contrib-type="author">
<name name-style="western"><surname>Zimasova</surname><given-names>Alsu</given-names></name>
<xref ref-type="aff" rid="aff-1">1</xref>
</contrib>
<contrib id="author-3" contrib-type="author">
<name name-style="western"><surname>Kozlov</surname><given-names>Nikolai</given-names></name>
<xref ref-type="aff" rid="aff-2">2</xref>
</contrib>
<aff id="aff-1"><label>1</label><institution>Laboratory of Vibrational Hydromechanics, Perm State Humanitarian Pedagogical University</institution>, <addr-line>Perm, 614990</addr-line>, <country>Russia</country></aff>
<aff id="aff-2"><label>2</label><institution>Institut de M&#x00E9;canique des Fluides de Toulouse</institution>, <addr-line>Toulouse INP, Toulouse, 31400</addr-line>, <country>France</country></aff>
</contrib-group><author-notes><corresp id="cor1"><label>&#x002A;</label>Corresponding Author: Victor Kozlov. Email: <email>kozlov@pspu.ru</email></corresp></author-notes>
<pub-date date-type="collection" publication-format="electronic">
<year>2024</year>
</pub-date>
<pub-date date-type="pub" publication-format="electronic">
<day>23</day><month>12</month><year>2024</year>
</pub-date>
<volume>20</volume>
<issue>12</issue>
<fpage>2693</fpage>
<lpage>2707</lpage>
<history>
<date date-type="received"><day>01</day><month>4</month><year>2024</year></date>
<date date-type="accepted"><day>18</day><month>6</month><year>2024</year></date>
</history>
<permissions>
<copyright-statement>&#x00A9; 2024 The Authors.</copyright-statement>
<copyright-year>2024</copyright-year>
<copyright-holder>Published by Tech Science Press.</copyright-holder>
<license xlink:href="https://creativecommons.org/licenses/by/4.0/">
<license-p>This work is licensed under a <ext-link ext-link-type="uri" xlink:type="simple" xlink:href="https://creativecommons.org/licenses/by/4.0/">Creative Commons Attribution 4.0 International License</ext-link>, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.</license-p>
</license>
</permissions>
<self-uri content-type="pdf" xlink:href="TSP_FDMP_52398.pdf"></self-uri>
<abstract>
<p>The behavior of a viscous liquid film on the wall of a rapidly rotating cylinder subjected to angular vibrations is experimentally studied. The cavity is filled with an immiscible low-viscosity liquid of lower density. In the absence of vibrations, the high viscosity liquid covers the inner surface of the cylinder with a relatively thin axisymmetric film; the low-viscosity liquid is located in the cavity interior. It is found that with an increase in the amplitude of rotational vibrations, the axisymmetric interphase boundary loses stability. An azimuthally periodic 2D &#x201C;frozen wave&#x201D; appears on the film surface in a threshold manner. It is shown that the frozen wave excitation is associated with the oscillatory Kelvin&#x2014;Helmholtz instability, and the stability threshold depends on a vibrational parameter. Two new vibrational effects in rotating cavities are studied accordingly: the stability (critical value of vibrational parameter) grows with decreasing the contrast in liquids viscosity; the rotation (the Coriolis force) stabilizes the interface&#x2013;the critical value of vibrational parameter grows with the dimensionless rotation rate, the threshold is characterized by the product of the aforementioned vibrational parameter and the dimensionless rotation rate to some power. The discovered phenomena can be useful for vibrational control of interfaces in many technological processes, especially in the field of materials science.</p>
</abstract>
<kwd-group kwd-group-type="author">
<kwd>Rotation</kwd>
<kwd>oscillations</kwd>
<kwd>immiscible fluids</kwd>
<kwd>interface</kwd>
<kwd>viscosity contrast</kwd>
<kwd>&#x201C;frozen wave&#x201D; instability</kwd>
</kwd-group>
<funding-group>
<award-group id="awg1">
<funding-source>Russian Science Foundation</funding-source>
<award-id>23-11-00242</award-id>
</award-group>
</funding-group>
</article-meta>
</front>
<body>
<sec id="s1">
<label>1</label>
<title>Introduction</title>
<p>The problem of the dynamics and stability of interphase boundaries is relevant in scientific and applied aspects [<xref ref-type="bibr" rid="ref-1">1</xref>,<xref ref-type="bibr" rid="ref-2">2</xref>]. The stability of rimming flows in rotating cavities is actual for fundamental science and is an important technological problem, the study of which has been the subject of many works [<xref ref-type="bibr" rid="ref-3">3</xref>&#x2013;<xref ref-type="bibr" rid="ref-7">7</xref>]. The instability of the interface can be excited by gravity in various rotating hydrodynamic systems, two low-viscosity immiscible liquids of different densities [<xref ref-type="bibr" rid="ref-8">8</xref>], and the surface of a granular medium in a liquid [<xref ref-type="bibr" rid="ref-9">9</xref>,<xref ref-type="bibr" rid="ref-10">10</xref>]. Of great interest in this regard is the effect of rotational vibration on the shape of the boundary discovered in [<xref ref-type="bibr" rid="ref-11">11</xref>]. It was found in [<xref ref-type="bibr" rid="ref-11">11</xref>] that when modulating the rotation speed of a cylindrical cavity containing two liquids, when the denser liquid covering the lateral boundary has a high viscosity, the interphase axisymmetric boundary loses stability. With an increase in the amplitude of the rotation speed modulation, a quasi-stationary relief in the form of a &#x201C;frozen&#x201D; wave appears on the interface in a threshold manner. The relief has the form of an azimuthally periodic system of two-dimensional crests and troughs extended along the axis of rotation, which are rotating together with the container and performing slight azimuthal oscillations relative to the cavity with the libration frequency. It was shown that the appearance of the frozen two-dimensional wave on the surface of a viscous liquid film is associated with the development of Kelvin&#x2013;Helmholtz oscillatory instability. The physical model proposed in [<xref ref-type="bibr" rid="ref-11">11</xref>], which describes the development of the frozen wave on the surface of the layer (film) of the viscous liquid on the inner wall of the rotating horizontal cylinder, is based on the results of systematic theoretical [<xref ref-type="bibr" rid="ref-12">12</xref>&#x2013;<xref ref-type="bibr" rid="ref-16">16</xref>] (and later [<xref ref-type="bibr" rid="ref-17">17</xref>]) and experimental [<xref ref-type="bibr" rid="ref-18">18</xref>&#x2013;<xref ref-type="bibr" rid="ref-20">20</xref>] studies of the Kelvin&#x2013;Helmholtz oscillatory instability without rotation. A feature of the cited works is that the instability of the plane interphase boundary is studied during tangential oscillations of liquids relative to the interface caused by translational vibrations. The experimental results [<xref ref-type="bibr" rid="ref-11">11</xref>] are in agreement with the model constructed, which reflects the behavior of the interphase boundary only to certain approximations. The latter include: relatively slow rotation, when the Coriolis force does not play a role; high viscosity of the liquid covering the cavity wall, when the entire layer of viscous liquid is completely entrained by the wall during its azimuthal oscillations; high-frequency modulation of the rotation speed, at which the low-viscosity liquid filling the remaining volume of the cavity rotates at a constant speed due to the absence of viscous interaction with the denser liquid. The latter means that the thickness of the Stokes layer in the low-viscosity liquid near the interface is negligibly thin due to the high contrast of liquid viscosities. Finally, the radius of the interface in the rotating cylinder is assumed large compared to the capillary length, while the length of the frozen wave is small compared to the azimuthal length of the interface. The above makes it relevant to study the influence, on the effect of excitation of the quasi-stationary relief at the boundary of the viscous-liquid layer during the non-monotonous rotation of the cavity, of such factors as: the thickness of the viscous liquid layer, the contrast of viscosities and the rotation speed of the cavity.</p>
<p>The relevance of the study of interface dynamics is determined by the importance of the fundamental and technological problem of controlling mass transfer across the interface [<xref ref-type="bibr" rid="ref-21">21</xref>,<xref ref-type="bibr" rid="ref-22">22</xref>]. At the same time, vibrational methods for controlling the interface dynamics are of particular interest due to the convenience and simplicity of the vibration effect on hydrodynamic systems [<xref ref-type="bibr" rid="ref-23">23</xref>,<xref ref-type="bibr" rid="ref-24">24</xref>]. Note that the effect of rotational vibrations (rotation rate modulation) on the shape of the interphase boundary, discovered experimentally in [<xref ref-type="bibr" rid="ref-11">11</xref>], is original and qualitatively new; the excitation of the oscillating motion of liquids near the interphase boundary in this case is determined by the different interactions of liquids with the boundaries of the cavity and with each other, due to high contrast of viscosities. At the same time, the experimental results and the physical model [<xref ref-type="bibr" rid="ref-11">11</xref>] refer to the case of relatively slow rotation, when rotation (Coriolis force) does not play an important role.</p>
<p>The present study is an advancement over [<xref ref-type="bibr" rid="ref-11">11</xref>]; the objective of this work is the experimental investigation of the dynamics of the boundary of a viscous-liquid layer with variations in the thickness of the viscous liquid layer and the rotation rate. The studies are performed with liquids of lower contrast of viscosities in a wide range of amplitudes and frequencies of rotation rate modulation with varying thicknesses of the viscous liquid layer. The novel and important result: it is found that the rotation has a stabilizing effect, which can be characterized by a dimensionless rotation rate, and the threshold of axisymmetric interface stability is determined by the product of vibrational parameter and the dimensionless rotation rate to some power.</p>
</sec>
<sec id="s2">
<label>2</label>
<title>Experimental Setup and Procedure</title>
<sec id="s2_1">
<label>2.1</label>
<title>Experimental Setup</title>
<p>The stability of the interface between two liquids in a horizontal long cylinder is studied experimentally for the case when the rotation velocity is modulated against a background of uniform rotation. The liquids are: low viscosity and low density PMS-5 silicone oil and more dense and viscous glycerol. The coefficient of interfacial tension at the PMS-5&#x2013;glycerol interface was measured using the hanging drop technique. The liquids properties as well as the viscosity contrast coefficient of liquids <inline-formula id="ieqn-1">
<mml:math id="mml-ieqn-1"><mml:mrow><mml:mi mathvariant="normal">K</mml:mi></mml:mrow><mml:mo>&#x2261;</mml:mo><mml:msqrt><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>1</mml:mn></mml:msub></mml:mrow></mml:msqrt></mml:math>
</inline-formula> are presented in <xref ref-type="table" rid="table-1">Table 1</xref>. The definition of the viscosity contrast coefficient corresponds to [<xref ref-type="bibr" rid="ref-14">14</xref>], in fact, this coefficient characterizes the ratio of the thicknesses of Stokes boundary layers in liquids.</p>
<table-wrap id="table-1"><label>Table 1</label>
<caption>
<title>Liquids properties</title></caption>
<table><colgroup>
<col/>
<col/>
<col/>
<col/>
<col/>
</colgroup>
<thead>
<tr>
<th>Liquid</th>
<th>Density (g/cm<sup>3</sup>)</th>
<th>Viscosity, (St)</th>
<th>Contrast of viscosities <inline-formula id="ieqn-2">
<mml:math id="mml-ieqn-2"><mml:mrow><mml:mi mathvariant="normal">K</mml:mi></mml:mrow><mml:mo>&#x2261;</mml:mo><mml:msqrt><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>1</mml:mn></mml:msub></mml:mrow></mml:msqrt></mml:math>
</inline-formula></th>
<th>Surface tension (g/s<sup>2</sup>)</th>
</tr>
</thead>
<tbody>
<tr>
<td rowspan="2">PMS-5 silicone oil&#x2013;Glycerol</td>
<td><inline-formula id="ieqn-3">
<mml:math id="mml-ieqn-3"><mml:mrow><mml:msub><mml:mi>&#x03C1;</mml:mi><mml:mn>1</mml:mn></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>0.92</mml:mn></mml:math>
</inline-formula></td>
<td><inline-formula id="ieqn-4">
<mml:math id="mml-ieqn-4"><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>1</mml:mn></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>0.053</mml:mn></mml:math>
</inline-formula></td>
<td rowspan="2">12</td>
<td rowspan="2"><inline-formula id="ieqn-5">
<mml:math id="mml-ieqn-5"><mml:mi>&#x03C3;</mml:mi><mml:mo>=</mml:mo><mml:mn>23.9</mml:mn></mml:math>
</inline-formula></td>
</tr>
<tr>
<td><inline-formula id="ieqn-6">
<mml:math id="mml-ieqn-6"><mml:mrow><mml:msub><mml:mi>&#x03C1;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>1.26</mml:mn></mml:math>
</inline-formula></td>
<td><inline-formula id="ieqn-7">
<mml:math id="mml-ieqn-7"><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>7.6</mml:mn></mml:math>
</inline-formula></td>
</tr>
<tr>
<td rowspan="2">[<xref ref-type="bibr" rid="ref-11">11</xref>] PMS-0.65 silicone oil&#x2013;Glycerol</td>
<td><inline-formula id="ieqn-8">
<mml:math id="mml-ieqn-8"><mml:mrow><mml:msub><mml:mi>&#x03C1;</mml:mi><mml:mn>1</mml:mn></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>0.76</mml:mn></mml:math>
</inline-formula></td>
<td><inline-formula id="ieqn-9">
<mml:math id="mml-ieqn-9"><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>1</mml:mn></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>0.010</mml:mn></mml:math>
</inline-formula></td>
<td rowspan="2">29</td>
<td rowspan="2"><inline-formula id="ieqn-10">
<mml:math id="mml-ieqn-10"><mml:mi>&#x03C3;</mml:mi><mml:mo>=</mml:mo><mml:mn>30.2</mml:mn></mml:math>
</inline-formula></td>
</tr>
<tr>
<td><inline-formula id="ieqn-11">
<mml:math id="mml-ieqn-11"><mml:mrow><mml:msub><mml:mi>&#x03C1;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>1.26</mml:mn></mml:math>
</inline-formula></td>
<td><inline-formula id="ieqn-12">
<mml:math id="mml-ieqn-12"><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>8.2</mml:mn></mml:math>
</inline-formula></td>
</tr>
</tbody>
</table>
</table-wrap>
<p>The experiments are carried out at a relatively rapid rotation of the cavity, when the entire system is in the centrifuged state, while the viscous heavy liquid under the influence of the centrifugal force is located near the cavity wall, forming an axisymmetric layer of thickness <italic>h</italic><sub>0</sub>, and the light, low-viscosity liquid is located in the center of the cavity in the form of a cylinder with a radius <italic>R</italic><sub><italic>in</italic></sub> (<xref ref-type="fig" rid="fig-1">Fig. 1</xref>). The experiments are carried out with the layers of viscous liquid of different thicknesses, <italic>h</italic><sub>0</sub> &#x003D; 3.3, 4.6 mm.</p>
<fig id="fig-1">
<label>Figure 1</label>
<caption>
<title>Scheme of the liquid distribution in the cavity cross section without librations</title></caption>
<graphic mimetype="image" mime-subtype="tif" xlink:href="FDMP_52398-fig-1.tif"/>
</fig>
<p>The results obtained are compared with the results of a similar experiment [<xref ref-type="bibr" rid="ref-11">11</xref>], performed with a pair of liquids silicone oil PMS-0.65&#x2013;glycerin, with a higher contrast of viscosities <inline-formula id="ieqn-13">
<mml:math id="mml-ieqn-13"><mml:mrow><mml:mi mathvariant="normal">K</mml:mi></mml:mrow><mml:mo>=</mml:mo><mml:mn>29</mml:mn></mml:math>
</inline-formula>. The liquid properties are also presented in <xref ref-type="table" rid="table-1">Table 1</xref>. The layer thickness in [<xref ref-type="bibr" rid="ref-11">11</xref>] was <italic>h</italic><sub>0</sub> &#x003D; 3.0 mm.</p>

<p>The experimental setup (<xref ref-type="fig" rid="fig-2">Fig. 2</xref>) is a horizontal cylindrical cavity with a radius <inline-formula id="ieqn-14">
<mml:math id="mml-ieqn-14"><mml:mi>R</mml:mi><mml:mspace width="thinmathspace" /><mml:mrow><mml:mo>=</mml:mo></mml:mrow><mml:mspace width="thinmathspace" /><mml:mrow><mml:mn>3</mml:mn></mml:mrow><mml:mrow><mml:mn>.0</mml:mn></mml:mrow></mml:math>
</inline-formula> cm and a length <inline-formula id="ieqn-15">
<mml:math id="mml-ieqn-15"><mml:mi>L</mml:mi><mml:mo>=</mml:mo><mml:mn>7.4</mml:mn></mml:math>
</inline-formula> cm. The cavity rotation according to the law <inline-formula id="ieqn-16">
<mml:math id="mml-ieqn-16"><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mo>=</mml:mo><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo stretchy="false">(</mml:mo><mml:mn>1</mml:mn><mml:mo>+</mml:mo><mml:mi>&#x03B5;</mml:mi><mml:mi>cos</mml:mi><mml:mo>&#x2061;</mml:mo><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mi>t</mml:mi><mml:mo stretchy="false">)</mml:mo></mml:math>
</inline-formula> is set by a stepper motor type FL86STH118-6004A. Here <inline-formula id="ieqn-17">
<mml:math id="mml-ieqn-17"><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula> is the rotation speed, <inline-formula id="ieqn-18">
<mml:math id="mml-ieqn-18"><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula>&#x2013;circular frequency of modulation, <inline-formula id="ieqn-19">
<mml:math id="mml-ieqn-19"><mml:mi>&#x03B5;</mml:mi></mml:math>
</inline-formula>&#x2013; dimensionless amplitude of rotation speed modulation. The cavity rotation rate varies in the range <inline-formula id="ieqn-20">
<mml:math id="mml-ieqn-20"><mml:mrow><mml:msub><mml:mi>f</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo>&#x2261;</mml:mo><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mn>2</mml:mn><mml:mi>&#x03C0;</mml:mi><mml:mo>=</mml:mo><mml:mn>3</mml:mn><mml:mo>&#x2212;</mml:mo><mml:mn>6</mml:mn><mml:mtext>&#x00A0;</mml:mtext></mml:math>
</inline-formula>rps, the frequency of the velocity modulation varies within <inline-formula id="ieqn-21">
<mml:math id="mml-ieqn-21"><mml:mrow><mml:msub><mml:mi>f</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo>&#x2261;</mml:mo><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mn>2</mml:mn><mml:mi>&#x03C0;</mml:mi><mml:mo>=</mml:mo><mml:mn>3</mml:mn><mml:mo>&#x2212;</mml:mo><mml:mn>7</mml:mn></mml:math>
</inline-formula> Hz and the amplitude of the rotation velocity modulation changes in the interval <inline-formula id="ieqn-22">
<mml:math id="mml-ieqn-22"><mml:mi>&#x03B5;</mml:mi><mml:mo>=</mml:mo><mml:mn>0</mml:mn><mml:mo>&#x2212;</mml:mo><mml:mn>0.9</mml:mn></mml:math>
</inline-formula>.</p>
<fig id="fig-2">
<label>Figure 2</label>
<caption>
<title>Scheme of the experimental setup</title></caption>
<graphic mimetype="image" mime-subtype="tif" xlink:href="FDMP_52398-fig-2.tif"/>
</fig>
<p>The cavity is machined inside a Plexiglas parallelepiped of square cross-section. The transparent flanges and polished edges of the cuvette allow liquids to be observed practically without optical distortion both from the end and from the side. A detailed description of the cuvette design can be found in [<xref ref-type="bibr" rid="ref-11">11</xref>]. When studying the shape of the interphase boundary in cross-section, the cuvette is illuminated with a green light sheet from a laser of the type KLM-532/h-1000 with the power of 1 W. The laser sheet thickness is 2 mm. The plane of the laser sheet is perpendicular to the axis of the cavity rotation. Taking into account the two-dimensionality of the vibration structures, the optimal position for the laser light sheet is selected to be on the median of the cavity length in experiments. To exclude the extraneous light the side walls of the cavity, except the slot for the light sheet, are covered with black self-adhesive film. The viscous liquid (glycerol) is visualized by rhodamine, which fluoresces red under the green laser light. The concentration of the dissolved rhodamine does not exceed 10<sup>&#x2212;3</sup> percent and its presence does not affect the physical properties of the liquid. Rhodamine does not dissolve in the low-viscosity liquid, which provides a high brightness contrast at the interface. The use of a red filter during the video recording of the interface eliminates the stray light and enhances the contrast of the boundary image.</p>
<p>Photo and video recording of the interface between two liquids is carried out through the front transparent end of the cavity using a high-speed video camera (type CamRecord Optronis CL600 &#x00D7; 2) installed coaxially with the axis of the cavity rotation. The images are captured with a resolution of 800 &#x00D7; 800 pix (and further processed using a computer), with a frame rate of 420 fps, sufficient to study the shape of the interphase boundary and its transformation during the period of velocity modulation.</p>
</sec>
<sec id="s2_2">
<label>2.2</label>
<title>Experimental Technique</title>
<p>The experiment begins with the cuvette being rapidly rotated (<inline-formula id="ieqn-23">
<mml:math id="mml-ieqn-23"><mml:mrow><mml:msub><mml:mi>f</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mtext>&#x00A0;</mml:mtext><mml:mo>&#x003E;</mml:mo><mml:mtext>&#x00A0;</mml:mtext><mml:mn>15</mml:mn><mml:mtext>&#x00A0;</mml:mtext></mml:math>
</inline-formula>rps) while the interface between the liquids takes an axisymmetric shape. Within a few tens of seconds, under the action of centrifugal force, the end surface is cleared of droplets of viscous (more dense) liquid. After this, the rotation velocity is gradually decreased to the required value <inline-formula id="ieqn-24">
<mml:math id="mml-ieqn-24"><mml:mrow><mml:msub><mml:mi>f</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula>. The observation of the boundary shape is carried out with a step-by-step increase in the amplitude of the velocity modulation at a given frequency <inline-formula id="ieqn-25">
<mml:math id="mml-ieqn-25"><mml:mrow><mml:msub><mml:mi>f</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula>. In <xref ref-type="fig" rid="fig-3">Fig. 3a</xref>, the interface is visible as a bright light line enclosed between dark stripes. The developed technique for visualizing one of the liquids (with higher refractive index) with rhodamine allows one to see the interface in the form of a thin line. The appearance of a dark stripe on the side of the viscous liquid layer is explained by the phenomenon of total internal reflection&#x2013;the refractive index of glycerin exceeds that of low-viscosity oil in the central part of the cavity.</p>
<fig id="fig-3">
<label>Figure 3</label>
<caption>
<title>Pictures of interface when modulating the rotation velocity at <italic>f</italic><sub><italic>rot</italic></sub> &#x003D; 3 rps, <italic>f</italic><sub><italic>lib</italic></sub> &#x003D; 4 Hz: <italic>a&#x2013;d</italic>) <italic>&#x03B5;</italic> &#x003D; 0; 0.52, 0.54, 0.56. Pictures of interface at <italic>f</italic><sub><italic>rot</italic></sub> &#x003D; 3 rps, <italic>f</italic><sub><italic>lib</italic></sub> &#x003D; 3 Hz: <italic>e&#x2013;f</italic>) <italic>&#x03B5;</italic> &#x003D; 0.45, 0.49. The blue line in <xref ref-type="fig" rid="fig-3">Fig. 3a</xref> shows the boundary of the cavity in the cross-sectional plane of the light sheet, working fluids are PMS-5 and glycerol, <italic>h</italic><sub>0</sub> &#x003D; 4.6 mm</title></caption>
<graphic mimetype="image" mime-subtype="tif" xlink:href="FDMP_52398-fig-3.tif"/>
</fig>
<p>It was found that with the increase in the amplitude of the rotation velocity modulation <italic>&#x03B5;</italic>, the axisymmetric interface loses its stability in a threshold manner, and a quasi-stationary two-dimensional relief with an azimuthal periodicity develops on it (<xref ref-type="fig" rid="fig-3">Fig. 3b</xref>&#x2013;<xref ref-type="fig" rid="fig-3">d</xref>). Two-dimensional crests of viscous liquid extended along the axis of rotation move together with the cavity. With the increase in the velocity modulation amplitude, the height of the frozen wave increases as well. The threshold value of the modulation amplitude <italic>&#x03B5;</italic> and the azimuthal wave number of the wave in the threshold depend on the rotation velocity and the velocity modulation frequency.</p>
<p>As noted above, in the subthreshold area the interface has an axisymmetric shape. It should be noted that if the frequency of librations <italic>f</italic><sub><italic>lib</italic></sub> coincides with the rotation velocity <italic>f</italic><sub><italic>rot</italic></sub> the interphase boundary loses axial symmetry before the Kelvin&#x2013;Helmholtz instability occurs: the boundary shifts from the rotation axis in the radial direction. The displacement increases with the velocity modulation amplitude. With a small displacement, the boundary retains a circular shape. As it approaches the boundary of the rotating cavity, the interphase boundary loses its circular shape (<xref ref-type="fig" rid="fig-3">Fig. 3e</xref>). A theoretical description of this effect is available in [<xref ref-type="bibr" rid="ref-25">25</xref>]. It was shown that the violation of the axial symmetry of the interphase boundary is associated with the average force field formed in the rotating reference frame by the action of the gravity field transverse to the axis of rotation. It should be noted that if the frequencies coincide, <inline-formula id="ieqn-26">
<mml:math id="mml-ieqn-26"><mml:mrow><mml:msub><mml:mi>f</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mrow><mml:msub><mml:mi>f</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula>, the development of the frozen wave instability is also observed upon reaching a certain threshold value of the libration amplitude <italic>&#x03B5;</italic>. The wave develops in a part of the boundary, which is limited to the area where the layer thickness is the smallest (<xref ref-type="fig" rid="fig-3">Fig. 3f</xref>). The present study is devoted to the stability of an axisymmetric unperturbed boundary, which is formed in the entire studied range of libration frequencies and rotation rates when the libration and rotation frequencies do not coincide. The study of the boundary dynamics, when the rotation velocity and the libration frequency coincide, is beyond the scope of this work.</p>
</sec>
</sec>
<sec id="s3">
<label>3</label>
<title>Experimental Results</title>
<sec id="s3_1">
<label>3.1</label>
<title>Interface Stability</title>
<p>The studies have shown that at small libration amplitudes, the boundary retains an axisymmetric shape. The threshold excitation of the wave relief in the studied range of parameters has a supercritical character&#x2013;the development of the wave with the increase in the modulation amplitude <inline-formula id="ieqn-27">
<mml:math id="mml-ieqn-27"><mml:mi>&#x03B5;</mml:mi></mml:math>
</inline-formula> and its disappearance while decreasing <inline-formula id="ieqn-28">
<mml:math id="mml-ieqn-28"><mml:mi>&#x03B5;</mml:mi></mml:math>
</inline-formula> occur without hysteresis. In most of the cases considered, with different <inline-formula id="ieqn-29">
<mml:math id="mml-ieqn-29"><mml:mrow><mml:msub><mml:mi>f</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula> and <italic>h</italic><sub>0</sub>, when increasing the frequency of librations, the threshold value of the modulation amplitude decreases (<xref ref-type="fig" rid="fig-4">Fig. 4a</xref>,<xref ref-type="fig" rid="fig-4">b</xref>). Only at the lowest rotation velocity, <italic>f</italic><sub><italic>rot</italic></sub> &#x003D; 3 rps, the stability threshold slightly varies with the libration frequency <italic>f</italic><sub><italic>lib</italic></sub>. A comparison to the results of the experiments [<xref ref-type="bibr" rid="ref-11">11</xref>] performed at <inline-formula id="ieqn-30">
<mml:math id="mml-ieqn-30"><mml:mrow><mml:mi mathvariant="normal">K</mml:mi></mml:mrow><mml:mo>=</mml:mo><mml:mn>29</mml:mn></mml:math>
</inline-formula> (<xref ref-type="fig" rid="fig-4">Fig. 4a</xref>) shows that the threshold curves [<xref ref-type="bibr" rid="ref-11">11</xref>] have a similar appearance, but are located higher. The confidence intervals for all points shown in <xref ref-type="fig" rid="fig-4">Fig. 4</xref> are <inline-formula id="ieqn-31">
<mml:math id="mml-ieqn-31"><mml:mi mathvariant="normal">&#x0394;</mml:mi><mml:mi>&#x03B5;</mml:mi><mml:mo>=</mml:mo><mml:mn>0.005</mml:mn></mml:math>
</inline-formula>, they are not presented so as not to clutter the picture. The confidence interval is determined by the step of <inline-formula id="ieqn-32">
<mml:math id="mml-ieqn-32"><mml:mi>&#x03B5;</mml:mi></mml:math>
</inline-formula> increase (decrease) during the experiment, which is 0.01; the threshold is determined by visually recognizing the appearance of relief. With increasing the thickness of the viscous liquid layer, the stability threshold grows (<xref ref-type="fig" rid="fig-4">Fig. 4b</xref>).</p>
<fig id="fig-4">
<label>Figure 4</label>
<caption>
<title>Stability threshold curves for an axisymmetric PMS-5&#x2013;glycerol boundary on the plane <inline-formula id="ieqn-33">
<mml:math id="mml-ieqn-33"><mml:mo stretchy="false">(</mml:mo><mml:mrow><mml:msub><mml:mi>f</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo>,</mml:mo><mml:mi>&#x03B5;</mml:mi><mml:mo stretchy="false">)</mml:mo></mml:math>
</inline-formula>: <italic>&#x0430;</italic>) <italic>h</italic><sub>0</sub> &#x003D; 3.3 mm&#x2013;empty points (for comparison the thresholds for the PMS-0.65&#x2013;glycerol pair are shown in filled symbols at <italic>h</italic><sub>0</sub> &#x003D; 3.0 mm [<xref ref-type="bibr" rid="ref-11">11</xref>]); <italic>b</italic>) <italic>h</italic><sub>0</sub> &#x003D; 4.6 mm. The dashed lines show the stability threshold when the libration frequency coincides with the rotation velocity</title></caption>
<graphic mimetype="image" mime-subtype="tif" xlink:href="FDMP_52398-fig-4.tif"/>
</fig>
<p>It is important to note that some points in <xref ref-type="fig" rid="fig-4">Fig. 4a</xref>,<xref ref-type="fig" rid="fig-4">b</xref> fall out of the monotonic dependencies corresponding to a given rotation velocity and are located significantly lower. These points correspond to the case when the libration frequency exactly coincides with the rotation velocity. If the frequency difference exceeds at least a few percent, this phenomenon does not appear. This displacement is due to the fact that when libration and rotation frequencies coincide, a loss of symmetry of the interphase boundary is observed (<xref ref-type="fig" rid="fig-3">Fig. 3&#x0435;</xref>). As a result of the boundary radial displacement the thickness of the viscous fluid layer decreases on a part of the perimeter. The loss of symmetry and the displacement of the interphase boundary occurs in a non-threshold manner and increases with the amplitude of the velocity modulation. Instability, in this case, is limited along the perimeter&#x2013;the frozen wave develops in the area where the layer has the smallest thickness (<xref ref-type="fig" rid="fig-3">Fig. 3f</xref>). It is interesting that the threshold points obtained in the layers of different initial thicknesses <italic>h</italic><sub>0</sub>, are consistent with each other. The local nature of the instability explains the agreement of the thresholds for different initial volumes of viscous liquid&#x2013;the threshold value is determined not by the average-along-layer thickness, but by the local one, which apparently takes on similar values at different fillings. As noted above, the object of this study is axisymmetric layers; the cases of frequency coincidence when the layers are not axisymmetric, will not be considered in further analysis and discussion.</p>
<p><xref ref-type="fig" rid="fig-5">Fig. 5</xref> shows the threshold values of the modulation amplitude depending on the libration frequency for different thicknesses of viscous liquid at different rotation velocities. It can be seen that with the increase in the layer thickness when going from <italic>h</italic><sub>0</sub> &#x003D; 3.3 mm to <italic>h</italic><sub>0</sub> &#x003D; 4.6 mm the threshold value increases. The comparison of the fragments <italic>&#x0430;</italic> and <italic>b</italic> (<xref ref-type="fig" rid="fig-5">Fig. 5</xref>) shows a decrease in the critical amplitude of the velocity modulation when increasing the rotation velocity. Note that the studied thicknesses meet the condition <inline-formula id="ieqn-34">
<mml:math id="mml-ieqn-34"><mml:mrow><mml:msub><mml:mi>h</mml:mi><mml:mn>0</mml:mn></mml:msub></mml:mrow><mml:mtext>&#x00A0;</mml:mtext><mml:mo>&#x003C;</mml:mo><mml:mtext>&#x00A0;</mml:mtext><mml:mrow><mml:msub><mml:mi>&#x03B4;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow></mml:math>
</inline-formula>, where <inline-formula id="ieqn-35">
<mml:math id="mml-ieqn-35"><mml:mrow><mml:msub><mml:mi>&#x03B4;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mo>&#x2261;</mml:mo><mml:msqrt><mml:mn>2</mml:mn><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:msqrt></mml:math>
</inline-formula> is the thickness of the Stokes layer in the viscous liquid. This limitation is due to the fact that the studied mechanism of the generation of an oscillating tangential velocity discontinuity [<xref ref-type="bibr" rid="ref-11">11</xref>] is based on the entrainment of a viscous fluid by the cavity wall performing rotational oscillations.</p>
<fig id="fig-5">
<label>Figure 5</label>
<caption>
<title>Dependence of the threshold value of the modulation amplitude <italic>&#x03B5;</italic> at the interface PMS-5&#x2013;glycerol on the frequency of librations at different thicknesses <italic>h</italic><sub>0</sub> for different rotation velocities <italic>f</italic><sub><italic>rot</italic></sub>: <italic>a</italic>)&#x2212;3 rps, <italic>b</italic>)&#x2212;5 rps. For comparison, the filled symbols show the results of experiments for the pair of liquids PMS-0.65&#x2013;glycerin [<xref ref-type="bibr" rid="ref-11">11</xref>]</title></caption>
<graphic mimetype="image" mime-subtype="tif" xlink:href="FDMP_52398-fig-5.tif"/>
</fig>
<p>The observations performed allow us to conclude that the stability threshold (threshold value of the velocity modulation amplitude): a) increases with the thickness of the viscous fluid layer; b) decreases with increasing the rotation velocity; c) decreases with the frequency of librations, and at high frequencies ceases to change. From a comparison with the results of [<xref ref-type="bibr" rid="ref-11">11</xref>], it follows that the contrast in liquid viscosities significantly changes the threshold value of the velocity modulation amplitude. At this, the rotation speed has a significant influence on the threshold. An explanation of the role of rotation speed and thickness of the viscous fluid layer will be given in paragraph 4, when analyzing the results in the space of the governing dimensionless parameters.</p>
</sec>
<sec id="s3_2">
<label>3.2</label>
<title>Shape of the Interphase Boundary</title>
<p>The observations show that in the supercritical area, the number of wavelengths over the perimeter of the interphase boundary takes on an integer value. The wavelength <italic>&#x03BB;</italic> is calculated based on the length of the unperturbed interface and the number of waves. In the supercritical region with the increase in the libration amplitude <italic>&#x03B5;</italic> (at constant values of the rotation velocity <italic>f</italic><sub><italic>rot</italic></sub> and the libration frequency <italic>f</italic><sub><italic>lib</italic></sub>) the length of the frozen wave remains practically unchanged in the studied range of parameters <italic>f</italic><sub><italic>rot</italic>,</sub>, <italic>f</italic><sub><italic>lib</italic></sub> and <italic>h</italic><sub>0</sub>.</p>
<p>The wavelength in the threshold of the instability development practically does not change with the frequency of librations (at a given rotation velocity) (<xref ref-type="fig" rid="fig-6">Fig. 6</xref>) in the area <italic>f</italic><sub><italic>lib</italic></sub> &#x003E; 4 Hz. At <italic>f</italic><sub><italic>lib</italic></sub> &#x003C; 4 Hz, a wave of greater length develops at the threshold. The large scatter of experimental points is due to the fact that an integer number of waves fits onto the perimeter, this means that the relative error of the measured wavelengths is more than 10 percent. At rotation speeds <italic>f</italic><sub>rot</sub> &#x003D; 4 and 5 rps, the wavelengths are consistent within experimental errors (represented in <xref ref-type="fig" rid="fig-6">Fig. 6</xref> by one curve, the lowest).</p>
<fig id="fig-6">
<label>Figure 6</label>
<caption>
<title>The wavelength <italic>&#x03BB;</italic> at the threshold of the relief appearance at the interface of PMS-5&#x2013;glycerol <italic>versus</italic> the frequency of librations <italic>f</italic><sub><italic>lib</italic></sub> at different rotation velocities <italic>f</italic><sub><italic>rot</italic></sub>, <italic>h</italic><sub>0</sub> &#x003D; 4.6 mm</title></caption>
<graphic mimetype="image" mime-subtype="tif" xlink:href="FDMP_52398-fig-6.tif"/>
</fig>
<p>At a fixed rotation velocity, the wavelength decreases while increasing the libration frequency (<xref ref-type="fig" rid="fig-7">Fig. 7</xref>).</p>
<fig id="fig-7">
<label>Figure 7</label>
<caption>
<title>Dependence of the wavelength <italic>&#x03BB;</italic> in the threshold of relief appearance on the interface PMS-0.65&#x2013;glycerol (solid symbols) and PMS-5&#x2013;glycerol on the frequency of librations at different thicknesses of the viscous liquid layer for rotation velocities <italic>f</italic><sub><italic>rot</italic></sub>: <italic>a</italic>) 3 rps, <italic>b</italic>) 5 rps</title></caption>
<graphic mimetype="image" mime-subtype="tif" xlink:href="FDMP_52398-fig-7.tif"/>
</fig>
<p><xref ref-type="fig" rid="fig-7">Fig. 7</xref> shows that at a given rotation speed, the results of measuring the wavelength of the azimuthal relief in layers of different thicknesses (3.3 and 4.6 mm) are consistent with an accuracy of scatter, associated, first of all, with the integer value of the waves falling on the perimeter. Thus, the thickness of the viscous liquid layer <italic>h</italic><sub>0</sub> has little effect on the wavelength. From a comparison of wavelengths at the glycerol&#x2013;PMS-0.65 interface [<xref ref-type="bibr" rid="ref-11">11</xref>] (presented by solid symbols in <xref ref-type="fig" rid="fig-7">Fig. 7</xref>) it follows that the wavelength at the threshold for this pair of liquids is less than at the boundary of the glycerol&#x2013;PMS-5 liquids. Thus, the contrast of liquids viscosities plays an important role. It should be noted that an increase in the rotation speed in all cases is accompanied by a decrease in the wavelength of the structures (compare fragments <italic>a</italic> and <italic>b</italic> in <xref ref-type="fig" rid="fig-7">Fig. 7</xref>).</p>
</sec>
</sec>
<sec id="s4">
<label>4</label>
<title>Analysis of Results</title>
<p>The appearance of a frozen wave at the interface is associated with the development of oscillatory Kelvin&#x2013;Helmholtz (K&#x2013;H) instability, excited by an oscillating tangential velocity discontinuity at the boundary. This phenomenon is known and studied experimentally and theoretically in the case of tangential oscillations of liquids relative to a flat interface. Such oscillations of liquids are excited, for example, under the action of horizontal translational harmonic oscillations of a cavity filled with liquids. Liquids of different densities oscillate along the interface in an oscillating inertial field. A theoretical model of this phenomenon was developed in [<xref ref-type="bibr" rid="ref-12">12</xref>] for non-viscous liquids. Subsequently, the stability of the interface between viscous liquids was examined theoretically and experimentally. In [<xref ref-type="bibr" rid="ref-14">14</xref>,<xref ref-type="bibr" rid="ref-16">16</xref>,<xref ref-type="bibr" rid="ref-19">19</xref>], it is shown that an increase in viscosity contrast leads to a significant decrease in the stability threshold.</p>
<p>In [<xref ref-type="bibr" rid="ref-11">11</xref>], the excitation of oscillatory instability was discovered in a non-uniformly rotating cylinder with two liquids with a high viscosity contrast. The rotation was carried out at a fairly high speed, and the system was in a centrifuged state with an axisymmetric interface. In this case, the more viscous liquid had a higher density and was located near the outer boundary of the cavity. The nature of the occurrence of an oscillating tangential velocity discontinuity at the interface between liquids was that the viscous liquid near the boundary of the cavity, with uneven rotation, was completely entrained by the cavity wall and performed rotational oscillations along with it, that is, the thickness of the liquid layer was less than the thickness of the Stokes layer. At the same time, the low-viscosity liquid in the middle part of the cavity rotated uniformly at a constant speed, since the Stokes boundary layers in it were of negligible thickness. The theoretical model built in [<xref ref-type="bibr" rid="ref-11">11</xref>], based on the results of studies in the case of translational oscillations [<xref ref-type="bibr" rid="ref-13">13</xref>,<xref ref-type="bibr" rid="ref-14">14</xref>,<xref ref-type="bibr" rid="ref-19">19</xref>], included the approximation <inline-formula id="ieqn-36">
<mml:math id="mml-ieqn-36"><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mtext>&#x00A0;</mml:mtext><mml:mo>&#x003C;&#x003C;</mml:mo><mml:mtext>&#x00A0;</mml:mtext><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula>; <inline-formula id="ieqn-37">
<mml:math id="mml-ieqn-37"><mml:mrow><mml:msub><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mo>&#x2261;</mml:mo><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:msubsup><mml:mi>h</mml:mi><mml:mn>0</mml:mn><mml:mn>2</mml:mn></mml:msubsup><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mtext>&#x00A0;</mml:mtext><mml:mo>&#x003C;&#x003C;</mml:mo><mml:mtext>&#x00A0;</mml:mtext><mml:mn>1</mml:mn></mml:math>
</inline-formula>, <inline-formula id="ieqn-38">
<mml:math id="mml-ieqn-38"><mml:mrow><mml:msub><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow><mml:mrow><mml:mn>1</mml:mn></mml:mrow></mml:msub></mml:mrow><mml:mo>&#x2261;</mml:mo><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:msubsup><mml:mi>h</mml:mi><mml:mn>0</mml:mn><mml:mn>2</mml:mn></mml:msubsup><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>1</mml:mn></mml:msub></mml:mrow><mml:mtext>&#x00A0;</mml:mtext><mml:mo>&#x003E;&#x003E;</mml:mo><mml:mtext>&#x00A0;</mml:mtext><mml:mn>1</mml:mn></mml:math>
</inline-formula>, <inline-formula id="ieqn-39">
<mml:math id="mml-ieqn-39"><mml:mrow><mml:msub><mml:mi>&#x03BB;</mml:mi><mml:mrow><mml:mi>c</mml:mi><mml:mi>a</mml:mi><mml:mi>p</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mtext>&#x00A0;</mml:mtext><mml:mo>&#x003C;&#x003C;</mml:mo><mml:mtext>&#x00A0;</mml:mtext><mml:mi>R</mml:mi></mml:math>
</inline-formula>. Thus, in the description of the phenomenon, the curvature of the surface is neglected (it is assumed that the wavelength is much less than the circumference), and the rotation speed is assumed to be small, that is, the effect of the Coriolis force is not taken into account. Note that in the described phenomenon, a high viscosity contrast (high viscosity of one of the liquids) plays a fundamental role, since it is the viscous liquid that performs tangential oscillations along the interface as a result of viscous drag by the oscillating wall.</p>
<p>The vibrational parameter B, which determines the threshold for the development of Kelvin&#x2013;Helmholtz oscillatory instability [<xref ref-type="bibr" rid="ref-12">12</xref>,<xref ref-type="bibr" rid="ref-13">13</xref>], is transformed under the conditions of the present problem. It characterizes the amplitude of the oscillating tangential velocity discontinuity at the interface between two fluids when one fluid oscillates relative to the other in an averaged centrifugal force field and, in accordance with [<xref ref-type="bibr" rid="ref-11">11</xref>], is determined by the expression</p>
<p><disp-formula id="eqn-1"><label>(1)</label>
<mml:math id="mml-eqn-1" display="block"><mml:mrow><mml:mi mathvariant="normal">B</mml:mi></mml:mrow><mml:mo>=</mml:mo><mml:mstyle displaystyle="true" scriptlevel="0"><mml:mrow><mml:mfrac><mml:mrow><mml:mi>&#x03C0;</mml:mi><mml:mi>&#x03C1;</mml:mi><mml:mrow><mml:msub><mml:mi>R</mml:mi><mml:mrow><mml:mi>i</mml:mi><mml:mi>n</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:msup><mml:mi>&#x03B5;</mml:mi><mml:mn>2</mml:mn></mml:msup></mml:mrow></mml:mrow><mml:mrow><mml:mn>2</mml:mn><mml:mo stretchy="false">(</mml:mo><mml:mn>1</mml:mn><mml:mo>&#x2212;</mml:mo><mml:mrow><mml:msup><mml:mi>&#x03C1;</mml:mi><mml:mn>2</mml:mn></mml:msup></mml:mrow><mml:mo stretchy="false">)</mml:mo><mml:mo stretchy="false">(</mml:mo><mml:mn>1</mml:mn><mml:mo>+</mml:mo><mml:mn>0.5</mml:mn><mml:mrow><mml:msup><mml:mi>&#x03B5;</mml:mi><mml:mn>2</mml:mn></mml:msup></mml:mrow><mml:mo stretchy="false">)</mml:mo><mml:mrow><mml:msub><mml:mi>&#x03BB;</mml:mi><mml:mrow><mml:mi>c</mml:mi><mml:mi>a</mml:mi><mml:mi>p</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:mrow></mml:mfrac></mml:mrow></mml:mstyle></mml:math>
</disp-formula>where, <inline-formula id="ieqn-40">
<mml:math id="mml-ieqn-40"><mml:mi>&#x03C1;</mml:mi><mml:mo>&#x2261;</mml:mo><mml:mstyle displaystyle="true" scriptlevel="0"><mml:mrow><mml:mfrac><mml:mrow><mml:mrow><mml:msub><mml:mi>&#x03C1;</mml:mi><mml:mn>1</mml:mn></mml:msub></mml:mrow></mml:mrow><mml:mrow><mml:mrow><mml:msub><mml:mi>&#x03C1;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow></mml:mrow></mml:mfrac></mml:mrow></mml:mstyle></mml:math>
</inline-formula>, <inline-formula id="ieqn-41">
<mml:math id="mml-ieqn-41"><mml:mrow><mml:msub><mml:mi>&#x03BB;</mml:mi><mml:mrow><mml:mi>c</mml:mi><mml:mi>a</mml:mi><mml:mi>p</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>2</mml:mn><mml:mi>&#x03C0;</mml:mi><mml:msqrt><mml:mstyle displaystyle="true" scriptlevel="0"><mml:mrow><mml:mfrac><mml:mi>&#x03C3;</mml:mi><mml:mrow><mml:mo stretchy="false">(</mml:mo><mml:mrow><mml:msub><mml:mi>&#x03C1;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mo>&#x2212;</mml:mo><mml:mrow><mml:msub><mml:mi>&#x03C1;</mml:mi><mml:mn>1</mml:mn></mml:msub></mml:mrow><mml:mo stretchy="false">)</mml:mo><mml:msubsup><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow><mml:mn>2</mml:mn></mml:msubsup><mml:mrow><mml:msub><mml:mi>R</mml:mi><mml:mrow><mml:mi>i</mml:mi><mml:mi>n</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo stretchy="false">(</mml:mo><mml:mn>1</mml:mn><mml:mo>+</mml:mo><mml:mn>0.5</mml:mn><mml:mrow><mml:msup><mml:mi>&#x03B5;</mml:mi><mml:mn>2</mml:mn></mml:msup></mml:mrow><mml:mo stretchy="false">)</mml:mo></mml:mrow></mml:mfrac></mml:mrow></mml:mstyle></mml:msqrt></mml:math>
</inline-formula>.</p>
<p>In this case, the role of the static force field in a rotating system is played by the centrifugal force averaged over the period, and the effect of the gravity field on the fluid in the cavity, which rotates quite rapidly relative to the horizontal axis, is neglected. Note that the results of experiments [<xref ref-type="bibr" rid="ref-11">11</xref>], carried out on liquids with a high viscosity contrast and on a relatively thin layer of viscous liquid, at high libration frequency were in satisfactory agreement with theoretical and experimental results for translational vibrations of the cavity in the absence of rotation [<xref ref-type="bibr" rid="ref-14">14</xref>,<xref ref-type="bibr" rid="ref-19">19</xref>].</p>
<p>The following questions remains: a) what is the role of the relative thickness of the viscous fluid layer, b) what role does the contrast of liquids viscosities play, c) how does the Coriolis force affect oscillatory K&#x2013;H instability in rotating cylinder. The dimensionless frequency <inline-formula id="ieqn-42">
<mml:math id="mml-ieqn-42"><mml:mrow><mml:msub><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow><mml:mn>2</mml:mn></mml:msub></mml:mrow><mml:mo>&#x2261;</mml:mo><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:msubsup><mml:mi>h</mml:mi><mml:mn>0</mml:mn><mml:mn>2</mml:mn></mml:msubsup><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>2</mml:mn></mml:msub></mml:mrow></mml:math>
</inline-formula> is responsible for the first point, which characterizes the ratio of the thickness of the viscous fluid layer to the thickness of the Stokes layer, and therefore the degree of entrainment of the viscous fluid layer by the oscillating wall. It is proposed to characterize the influence of the Coriolis force by the dimensionless rotation speed <inline-formula id="ieqn-43">
<mml:math id="mml-ieqn-43"><mml:mrow><mml:msub><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo>&#x2261;</mml:mo><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:msubsup><mml:mi>h</mml:mi><mml:mn>0</mml:mn><mml:mn>2</mml:mn></mml:msubsup><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>1</mml:mn></mml:msub></mml:mrow></mml:math>
</inline-formula>, this parameter characterizes the ratio of the Coriolis force to viscous forces (in this form&#x2013;in a layer of low-viscosity fluid).</p>
<p>By analogy with [<xref ref-type="bibr" rid="ref-11">11</xref>], we will plot the dependence of the threshold value of the vibration parameter B on the relative frequency of librations <inline-formula id="ieqn-44">
<mml:math id="mml-ieqn-44"><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula> (<xref ref-type="fig" rid="fig-8">Fig. 8</xref>). The figure shows that the stability threshold (critical value of parameter B) at a given rotation speed decreases with the relative frequency of librations <inline-formula id="ieqn-45">
<mml:math id="mml-ieqn-45"><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula> in all cases. At the same time, in a separate series of experiments performed on a layer of viscous liquid of a fixed thickness, the threshold curves are stratified by rotation speed; with increasing <italic>f</italic><sub><italic>rot</italic></sub>, the threshold curves rise, maintaining their shape.</p>
<fig id="fig-8">
<label>Figure 8</label>
<caption>
<title>Dependence of the threshold value of parameter B on the relative frequency of librations: <italic>a</italic>) <italic>h</italic><sub>0</sub> &#x003D; 3.3 mm (light symbols); <italic>b</italic>) <italic>h</italic><sub>0</sub> &#x003D; 4.6 mm; the results were obtained on a pair of liquids: glycerin&#x2013;PMS-5 with a viscosity contrast of K &#x003D; 12. In fragment <italic>a</italic>, dark symbols show the results [<xref ref-type="bibr" rid="ref-11">11</xref>] obtained on pair: glycerol&#x2013;PMS-0.65; K &#x003D; 29, <italic>h</italic><sub>0</sub> &#x003D; 3.0 mm</title></caption>
<graphic mimetype="image" mime-subtype="tif" xlink:href="FDMP_52398-fig-8.tif"/>
</fig>
<p>Comparison with the results of [<xref ref-type="bibr" rid="ref-11">11</xref>], obtained on a pair of liquids &#x201C;glycerol&#x2013;PMS-0.65&#x201D;, indicates that reducing the viscosity contrast increases stability (<xref ref-type="fig" rid="fig-8">Fig. 8</xref>). An increase in the thickness of viscous liquid layer is also accompanied by an increase in stability; with an increase in the layer thickness <italic>h</italic><sub>0</sub> &#x003D; 3.3 mm (<xref ref-type="fig" rid="fig-8">Fig. 8a</xref>) to <italic>h</italic><sub>0</sub> &#x003D; 4.6 mm (<xref ref-type="fig" rid="fig-8">Fig. 8b</xref>), the family of curves corresponding to different rotation speeds shifts upward. With relatively slow rotation <inline-formula id="ieqn-46">
<mml:math id="mml-ieqn-46"><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mtext>&#x00A0;</mml:mtext><mml:mo>&#x003E;</mml:mo><mml:mtext>&#x00A0;</mml:mtext><mml:mn>2</mml:mn></mml:math>
</inline-formula>, the stability threshold ceases to change with the relative frequency of librations. Note that in <xref ref-type="fig" rid="fig-8">Fig. 8</xref>, the points in case of libration and rotation frequencies coincidence, at <inline-formula id="ieqn-47">
<mml:math id="mml-ieqn-47"><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>1</mml:mn></mml:math>
</inline-formula>, fall out of the monotonic dependences and locate significantly lower.</p>
<p>The dimensionless wavelength &#x03BB;/&#x03BB;<sub><italic>cap</italic></sub>, as can be seen from <xref ref-type="fig" rid="fig-9">Fig. 9</xref>, at close values of <italic>h</italic><sub>0</sub> depends on the contrast of liquid viscosities: &#x03BB;/&#x03BB;<sub><italic>cap</italic></sub> goes up with the viscosity contrast. The dependences obtained for different pairs of liquids have a similar shape. It should be noted that a significant scatter of experimental points is determined by the condition of an integer number of waves falling on the perimeter of the interface.</p>
<fig id="fig-9">
<label>Figure 9</label>
<caption>
<title>Dimensionless parameter &#x03BB;/&#x03BB;<sub><italic>cap</italic></sub> <italic>versus</italic> the relative frequency of librations, PMS-5&#x2013;glycerol; for comparison, results of [<xref ref-type="bibr" rid="ref-11">11</xref>]: PMS-0.65&#x2013;glycerol</title></caption>
<graphic mimetype="image" mime-subtype="tif" xlink:href="FDMP_52398-fig-9.tif"/>
</fig>
<p>From <xref ref-type="fig" rid="fig-9">Fig. 9</xref>, it follows that for each pair of liquids, the points obtained at similar thicknesses fit within one dependence within the error. In the case of K &#x003D; 12 the curve lies higher than with K &#x003D; 29. It is worth noting that at low values of rotation speed, the dimensionless wavelength ceases to change, and the value of &#x03BB;/&#x03BB;<sub><italic>cap</italic></sub> approaches a value close to unity. This value agrees satisfactorily with the theoretical one in the case of translational oscillations of liquids (thick layers) near a flat boundary [<xref ref-type="bibr" rid="ref-12">12</xref>,<xref ref-type="bibr" rid="ref-14">14</xref>].</p>
<p>Let us dwell on the stratification of the threshold curves (<xref ref-type="fig" rid="fig-8">Fig. 8</xref>) by rotation speed (dependence of the stability threshold on the rotation speed)&#x2013;with increasing rotation speed, the threshold curves shift to the region of higher values of the vibrational parameter B. As noted above, the physical model of the development of oscillatory Kelvin&#x2013;Helmholtz instability does not take into account the action of the Coriolis force. Let us use the dimensionless rotation speed <inline-formula id="ieqn-48">
<mml:math id="mml-ieqn-48"><mml:mrow><mml:msub><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:msubsup><mml:mi>h</mml:mi><mml:mn>0</mml:mn><mml:mn>2</mml:mn></mml:msubsup><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi>&#x03BD;</mml:mi><mml:mn>1</mml:mn></mml:msub></mml:mrow></mml:math>
</inline-formula>, which characterizes the ratio of the thickness of the layer of a viscous liquid to the thickness of the Ekman layer in a low-viscosity liquid (more precisely, the square of this ratio) in a rotating cavity. From the analysis of the results obtained, it follows that the stabilizing effect of rotation on the stability of the interphase boundary in the experiment has a power-law dependence, and the stability threshold can be described by the complex <inline-formula id="ieqn-49">
<mml:math id="mml-ieqn-49"><mml:mrow><mml:mi mathvariant="normal">B</mml:mi></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:msubsup><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow><mml:mrow><mml:mn>0.35</mml:mn></mml:mrow></mml:msubsup></mml:math>
</inline-formula> (<xref ref-type="fig" rid="fig-10">Fig. 10</xref>).</p>
<fig id="fig-10">
<label>Figure 10</label>
<caption>
<title>Threshold of the interphase stability on the parameters plane, relative frequency of librations&#x2013;dimensionless complex <inline-formula id="ieqn-50">
<mml:math id="mml-ieqn-50"><mml:mrow><mml:mi mathvariant="normal">B</mml:mi></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:msubsup><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow><mml:mrow><mml:mn>0.35</mml:mn></mml:mrow></mml:msubsup></mml:math>
</inline-formula>, for pairs of liquids with different viscosity contrasts, PMS-5&#x2013;glycerin (K &#x003D; 12, present study) and PMS-0.65&#x2013;glycerin (K &#x003D; 29, [<xref ref-type="bibr" rid="ref-11">11</xref>])</title></caption>
<graphic mimetype="image" mime-subtype="tif" xlink:href="FDMP_52398-fig-10.tif"/>
</fig>
<p>All points obtained at different rotation speeds and stratified in <xref ref-type="fig" rid="fig-8">Fig. 8</xref> are in satisfactory agreement on the plane of these parameters (<xref ref-type="fig" rid="fig-10">Fig. 10</xref>) (symbols in <xref ref-type="fig" rid="fig-8">Figs. 8</xref> and <xref ref-type="fig" rid="fig-10">10</xref> coincide). This indicates that rotation has a stabilizing effect on the stability of the interphase boundary, and the stabilizing effect could be characterized by dimensionless rotation speed <inline-formula id="ieqn-51">
<mml:math id="mml-ieqn-51"><mml:mrow><mml:msub><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula>.</p>
<p>The threshold points are located much lower at <inline-formula id="ieqn-52">
<mml:math id="mml-ieqn-52"><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>1</mml:mn></mml:math>
</inline-formula>. This is explained by the fact that at this the frozen waves excite only on a part of the interphase boundary, where the layer thickness is much smaller than <italic>h</italic><sub>0</sub>, which means that the dimensionless rotation speed, being calculated through the local thickness of the viscous liquid layer, is also smaller. This could explain the decrease in the threshold value of <inline-formula id="ieqn-53">
<mml:math id="mml-ieqn-53"><mml:mrow><mml:mi mathvariant="normal">B</mml:mi></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:msubsup><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow><mml:mrow><mml:mn>0.35</mml:mn></mml:mrow></mml:msubsup></mml:math>
</inline-formula> at <inline-formula id="ieqn-54">
<mml:math id="mml-ieqn-54"><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mo>=</mml:mo><mml:mn>1</mml:mn></mml:math>
</inline-formula>.</p>
</sec>
<sec id="s5">
<label>5</label>
<title>Conclusion</title>
<p>The behavior of a viscous liquid film on the wall of rapidly rotating cylinder subjected to angular vibrations is experimentally studied. The cavity is filled with an immiscible low-viscosity liquid of lower density. It is found that with an increase in the amplitude of rotational vibrations, the axisymmetric interphase boundary loses stability&#x2013;&#x0430; periodic 2D frozen wave appears on the liquid-film interface in a threshold manner. The frozen wave excitation is associated with the oscillatory Kelvin&#x2013;Helmholtz instability, and the stability threshold is determined by vibrational parameter. The experiments carried out allow us to draw two important conclusions. The first concerns the role of the viscosity contrast coefficient K, which characterizes the ratio of the thicknesses of Stokes layers in liquids on opposite sides of the interface. It is shown that as the viscosity contrast decreases, the threshold for excitation of instability increases. This conclusion is qualitatively consistent with the results of theoretical and experimental studies of the oscillatory instability of the K&#x2013;H in plane geometry [<xref ref-type="bibr" rid="ref-14">14</xref>] in a different formulation: the layers of the liquid are considered thick, there is no rotation, and tangential oscillations of liquids are caused by uniform oscillating external force fields. The second important result concerns the role of cavity rotation. It was discovered that rotation plays a stabilizing role and leads to an increase in the threshold value of the vibrational parameter <inline-formula id="ieqn-55">
<mml:math id="mml-ieqn-55"><mml:mrow><mml:msup><mml:mrow><mml:mi mathvariant="normal">B</mml:mi></mml:mrow><mml:mrow><mml:mo>&#x2217;</mml:mo></mml:mrow></mml:msup></mml:mrow></mml:math>
</inline-formula> (at a given relative frequency of librations) according to a power law <inline-formula id="ieqn-56">
<mml:math id="mml-ieqn-56"><mml:mrow><mml:msup><mml:mrow><mml:mi mathvariant="normal">B</mml:mi></mml:mrow><mml:mrow><mml:mo>&#x2217;</mml:mo></mml:mrow></mml:msup></mml:mrow><mml:mo>&#x223C;</mml:mo><mml:msubsup><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow><mml:mi>n</mml:mi></mml:msubsup></mml:math>
</inline-formula>. Under the conditions of the experiments performed (at sufficiently high values of the viscosity contrast K &#x003D; 12 and K &#x003D; 29) <inline-formula id="ieqn-57">
<mml:math id="mml-ieqn-57"><mml:mi>n</mml:mi><mml:mo>&#x2248;</mml:mo><mml:mn>0.35</mml:mn></mml:math>
</inline-formula>. The use of a dimensionless complex <inline-formula id="ieqn-58">
<mml:math id="mml-ieqn-58"><mml:msubsup><mml:mrow><mml:mi mathvariant="normal">B</mml:mi><mml:mrow><mml:mo>/</mml:mo></mml:mrow><mml:mi>&#x03C9;</mml:mi></mml:mrow><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow><mml:mrow><mml:mn>0.35</mml:mn></mml:mrow></mml:msubsup></mml:math>
</inline-formula> makes it possible to coordinate experimental points obtained at different rotation speeds at a certain value of the contrast in liquid viscosities. Note that the found dependence well approximates the results of the present experiments. At the same time, one can expect a transformation of the dependence (in particular, the exponent <italic>n</italic>) with a change in K.</p>
<p>The results obtained shed light on the features of a new phenomenon discovered in [<xref ref-type="bibr" rid="ref-11">11</xref>]&#x2013;instability of the interface between liquids with a high contrast of viscosities in a cylindrical cavity undergoing modulated rotation. The discovered stabilizing effect of dimensionless rotation rate on the oscillatory instability of the interface is qualitatively new and promising in terms of applied development of vibrational methods for controlling the interfaces; it requires further systematic experimental and theoretical research. To develop this direction, the following is planned: a systematic experimental study of the dynamics of the interface depending on the relative volume of liquids and their properties with the viscosity contrast and dimensionless rotation speed variation; theoretical modeling of the found phenomenon.</p>
</sec>
</body>
<back>
<glossary content-type="abbreviations" id="glossary-1">
<title>Nomenclature</title>
<def-list>
<def-item>
<term><italic>R</italic></term>
<def>
<p>Cavity radius, m</p>
</def>
</def-item>
<def-item>
<term><italic>R</italic><sub>in</sub></term>
<def>
<p>Interface radius, m</p>
</def>
</def-item>
<def-item>
<term><italic>h</italic><sub>0</sub></term>
<def>
<p>Viscous liquid layer thickness, m</p>
</def>
</def-item>
<def-item>
<term><inline-formula id="ieqn-59">
<mml:math id="mml-ieqn-59"><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula></term>
<def>
<p>Rotation speed, s<sup>&#x2212;1</sup></p>
</def>
</def-item>
<def-item>
<term><inline-formula id="ieqn-60">
<mml:math id="mml-ieqn-60"><mml:mrow><mml:msub><mml:mi mathvariant="normal">&#x03A9;</mml:mi><mml:mrow><mml:mi>l</mml:mi><mml:mi>i</mml:mi><mml:mi>b</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula></term>
<def>
<p>Libration radian frequency, s<sup>&#x2212;1</sup></p>
</def>
</def-item>
<def-item>
<term><inline-formula id="ieqn-61">
<mml:math id="mml-ieqn-61"><mml:mi>&#x03B5;</mml:mi></mml:math>
</inline-formula></term>
<def>
<p>Amplitude of rotation speed modulation</p>
</def>
</def-item>
<def-item>
<term><inline-formula id="ieqn-62">
<mml:math id="mml-ieqn-62"><mml:mi>&#x03BB;</mml:mi></mml:math>
</inline-formula></term>
<def>
<p>Wavelength of &#x201C;frozen&#x201D; relief, m</p>
</def>
</def-item>
<def-item>
<term><inline-formula id="ieqn-63">
<mml:math id="mml-ieqn-63"><mml:mrow><mml:msub><mml:mi>&#x03BB;</mml:mi><mml:mrow><mml:mi>c</mml:mi><mml:mi>a</mml:mi><mml:mi>p</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula></term>
<def>
<p>Capillary wavelength, m</p>
</def>
</def-item>
<def-item>
<term><inline-formula id="ieqn-64">
<mml:math id="mml-ieqn-64"><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow></mml:math>
</inline-formula></term>
<def>
<p>Dimensionless libration frequency</p>
</def>
</def-item>
<def-item>
<term>B</term>
<def>
<p>Dimensionless vibrational parameter</p>
</def>
</def-item>
<def-item>
<term><inline-formula id="ieqn-65">
<mml:math id="mml-ieqn-65"><mml:mrow><mml:msub><mml:mrow><mml:mrow><mml:mi mathvariant="normal">&#x03C9;</mml:mi></mml:mrow></mml:mrow><mml:mrow><mml:mi>r</mml:mi><mml:mi>o</mml:mi><mml:mi>t</mml:mi></mml:mrow></mml:msub></mml:mrow></mml:math>
</inline-formula></term>
<def>
<p>Dimensionless rotation speed</p>
</def>
</def-item>
<def-item>
<term>K</term>
<def>
<p>Viscosity contrast coefficient</p>
</def>
</def-item>
</def-list>
</glossary>
<ack>
<p>The authors thank A.S. Selyanin for his help in experimental setup production.</p>
</ack>
<sec>
<title>Funding Statement</title>
<p>Victor Kozlov and Alsu Zimasova were financially supported by the Russian Science Foundation (Project 23-11-00242), Nikolai Kozlov had no specific support.</p>
</sec>
<sec>
<title>Author Contributions</title>
<p>The authors confirm contribution to the paper as follows: study conception and design: Victor Kozlov and Nikolai Kozlov; data collection: Alsu Zimasova; analysis and interpretation of results: Victor Kozlov, Alsu Zimasova and Nikolai Kozlov; draft manuscript preparation: Victor Kozlov, Alsu Zimasova and Nikolai Kozlov. All authors reviewed the results and approved the final version of the manuscript.</p>
</sec>
<sec sec-type="data-availability">
<title>Availability of Data and Materials</title>
<p>The data that support the findings of this study are available from the corresponding author.</p>
</sec>
<sec sec-type="COI-statement">
<title>Conflicts of Interest</title>
<p>The authors declare no conflicts of interest to report regarding the present study.</p>
</sec>
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